Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
7-Aminoindole → HCID 178527228, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 7-Aminoindole | HCID 111634 | — |
| 반응물 | 4-Sulfamoylbenzene-1-sulfonyl chloride | HCID 10956159 | — |
| 생성물 | HCID 178527228 | HCID 178527228 | 69.4% |
반응 단계
767 mg (3.0 mmol) of 4-sulfamoylbenzenesulfonyl chloride was reacted with 264 mg (2.0 mmol) of 7-amino-1H-indole and treated, to give 445 mg of N-(1H-indole-7-yl)-4-sulfanoylbenzenesulfonamide. The resulting compound was chlorinated using N-chlorosuccinimide in dichloromethane, to give 349 mg of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07834049B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-d24f49b68bf944d79c2e8a820fc732a0 |
| 출처 메모 | uspto-grants-2010_11 |