p-Fluoronitrobenzene → HCID 68427704, 화합물

반응식

[NH:1]1[CH2:5][CH2:4][CH:3]2[NH:6][CH2:7][CH2:8][CH:2]12.F[C:10]1[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][CH:11]=1>>[N+:16]([C:13]1[CH:14]=[CH:15][C:10]([N:1]2[CH2:5][CH2:4][CH:3]3[NH:6][CH2:7][CH2:8][CH:2]23)=[CH:11][CH:12]=1)([O-:18])=[O:17]

참가 물질

반응물 2

HCID 9590p-Fluoronitrobenzene

HCID 15106927HCID 15106927, 화합물

생성물 1

HCID 68427704HCID 68427704, 화합물

실험 절차

Octahydropyrrolo[3,2-b]pyrrole (0.50 g) was reacted by method C with 4-fluoronitrobenzene (0.53 g). The product with the molecular weight of 233.27 (C12H15N3O2); MS (ESI): 234 (M+H+) was obtained in this way.

후처리

customMS (ESI): 234 (M+H+) was obtained in this way

출처 및 근거

ORD 기록: ord-7cca1d61fd9c4647b5fcf933ee14a2cb
출처 데이터셋: uspto-grants-2010_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07838547B2

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