Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) → Methyl-(2-morpholin-4-yl-ethyl)-(6-nitro-benzothiazol-2-yl)-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) | HCID 77210 | — |
| 반응물 | N-Methyl-6-nitrobenzo[D]thiazol-2-amine | HCID 638568 | — |
| 생성물 | Methyl-(2-morpholin-4-yl-ethyl)-(6-nitro-benzothiazol-2-yl)-amine | HCID 57771793 | — |
반응 단계
The title compound is prepared according to the general procedure outlined in Example 61, Step 2, utilizing methyl-(6-nitro-benzothiazol-2-yl)-amine (1.18 g, 5.64 mmol) and N-(2-chloroethyl)-morpholine hydrochloride (2.45 g, 13.17 mmol) to yield 1.43 g (79%) of the product. mass spectrum (ion-spray): (m/z)=323.2 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07838543B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-b1c1071765a44a038f29f75c10dc9a97 |
| 출처 메모 | uspto-grants-2010_11 |