Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine, 1-(2-chloroethyl)-, hydrochloride → Methyl-(6-nitro-benzothiazol-2-yl)-(2-piperidin-1-yl-ethyl)-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine, 1-(2-chloroethyl)-, hydrochloride | HCID 74826 | — |
| 반응물 | N-Methyl-6-nitrobenzo[D]thiazol-2-amine | HCID 638568 | — |
| 생성물 | Methyl-(6-nitro-benzothiazol-2-yl)-(2-piperidin-1-yl-ethyl)-amine | HCID 57771692 | — |
반응 단계
The title compound is prepared according to the general procedure outlined in Example 61, Step 2, utilizing methyl(6-nitro-benzothiazol-2-yl)-amine (979 mg, 4.68 mmol) and N-(2-chloroethyl)-piperidine hydrochloride (2.01 g, 10.92 mmol) to yield 1.43 g (79%) of the product. mass spectrum (ion-spray): (m/z)=321.3 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07838543B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-bc555665845446f3bc46efa0a9d15277 |
| 출처 메모 | uspto-grants-2010_11 |