참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | (E)-1,3-Dichloropropene | HCID 24726 | — |
| 반응물 | N-Methyl-N-naphthylmethylamine | HCID 84474 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | (E)-3-Chloro-N-methyl-N-(1-naphthylmethyl)-2-propen-1-amine | HCID 9834733 | — |
반응 단계
30 g (0.175 mol) N-methyl-1-naphthalene methanamine, 100 ml MEK and 29 g (0.210 mol, 1.2 eq.) potassium carbonate are introduced into a reactor, the mixture is heated to 50° C. and 22.4 g (0.202 mol, 1.1 eq.) of (1E)-1,3-dichloro-1-propene added dropwise.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07838704B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_11 |
|---|
| ORD ID | ord-449e0bb65a6b42839560eb577a526773 |
|---|
| 출처 메모 | uspto-grants-2010_11 |
|---|
