Sulfamide → 3-Oxopiperazine-1-sulfonamide

반응식

[O:1]=[C:2]1[CH2:7][NH:6][CH2:5][CH2:4][NH:3]1.[S:8](N)([NH2:11])(=[O:10])=[O:9]>>[O:1]=[C:2]1[NH:3][CH2:4][CH2:5][N:6]([S:8]([NH2:11])(=[O:10])=[O:9])[CH2:7]1

참가 물질

반응물 2

HCID 82267Sulfamide

HCID 231360Piperazin-2-one

생성물 1

HCID 431320453-Oxopiperazine-1-sulfonamide

실험 절차

The subtitle compound was prepared according to the procedure outlined in Example 62 step i) using 2-oxopiperazine (0.5 g) and sulfamide (0.45 g) to give a beige solid. Yield: 0.83 g.

후처리

customto give a beige solid

출처 및 근거

ORD 기록: ord-64d1b96b651d41e6b459ab941b0e7141
출처 데이터셋: uspto-grants-2010_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07838675B2

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