Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl isocyanate → HCID 178418694, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl isocyanate | HCID 76639 | — |
| 반응물 | HCID 178419058 | HCID 178419058 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 178418694 | HCID 178418694 | 19.1% |
반응 단계
A solution of 4-(2-furyl)-1H-pyrrolo[2,3-d]pyrimidine-2-amine (192 mg, 0.96 mmol) in THF (3 mL) was treated with benzyl isocyanate (118 μL, 0.96 mmol), stirred at room temperature for 16 h and the resulting solid filtered and washed with EtOAc to give the title compound (61 mg, 19%) as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07098333B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-e3a6e51d909246489019c19083530959 |
| 출처 메모 | uspto-grants-2006_08 |