Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → N-(3-methoxyphenyl)-N'-[1-(2-nitrophenyl)ethylidene]hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | 2-Nitro-1-phenylethanone | HCID 94833 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 반응물 | 3-Methoxyphenylhydrazine hydrochloride | HCID 2723940 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(3-methoxyphenyl)-N'-[1-(2-nitrophenyl)ethylidene]hydrazine | HCID 74019072 | — |
반응 단계
A mixture of 3-methoxyphenylhydrazine hydrochloride (1.75 g), 2-nitroacetophenone (1.65 g), sodium acetate (0.82 g) and acetic acid (10 ml) was stirred at room temperature for 4 days. To the reaction mixture was added water, extracted with ethyl acetate. The extract was washed with water, brine, dried over anhydrous magnesium sulfate. The solvent was distilled off under reduced pressure to obtain the target compound (2.72 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07842701B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-573261e1a46940b09dc4e699d60da9d2 |
| 출처 메모 | uspto-grants-2010_11 |