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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1175799생성일: 2026년 10월 26일

Acetic Acid → N-(3-methoxyphenyl)-N'-[1-(2-nitrophenyl)ethylidene]hydrazine

https://huagongshe.com/reaction/1175799

반응식

참여 물질

역할이름HCID투입량
반응물Acetic AcidHCID 176—
반응물2-Nitro-1-phenylethanoneHCID 94833—
반응물Sodium AcetateHCID 517045—
반응물3-Methoxyphenylhydrazine hydrochlorideHCID 2723940—
용매WaterHCID 962—
생성물N-(3-methoxyphenyl)-N'-[1-(2-nitrophenyl)ethylidene]hydrazineHCID 74019072—

반응 단계

A mixture of 3-methoxyphenylhydrazine hydrochloride (1.75 g), 2-nitroacetophenone (1.65 g), sodium acetate (0.82 g) and acetic acid (10 ml) was stirred at room temperature for 4 days. To the reaction mixture was added water, extracted with ethyl acetate. The extract was washed with water, brine, dried over anhydrous magnesium sulfate. The solvent was distilled off under reduced pressure to obtain the target compound (2.72 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07842701B2
출처 데이터셋uspto-grants-2010_11
ORD IDord-573261e1a46940b09dc4e699d60da9d2
출처 메모uspto-grants-2010_11