1-Chloro-3-methoxypropane → 1-Ethoxy-2-(3-methoxypropoxy)-4-methylbenzene

반응식

[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH3:10])=[CH:6][C:5]=1[OH:11])[CH3:2].Cl[CH2:13][CH2:14][CH2:15][O:16][CH3:17]>>[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH3:10])=[CH:6][C:5]=1[O:11][CH2:13][CH2:14][CH2:15][O:16][CH3:17])[CH3:2]

참가 물질

반응물 2

HCID 1189271-Chloro-3-methoxypropane

HCID 122571232-Ethoxy-5-methylphenol

생성물 1

HCID 592240741-Ethoxy-2-(3-methoxypropoxy)-4-methylbenzene

실험 절차

Analogously to Method F, 5.05 g of 2-ethoxy-5-methylphenol and 4.03 g of 1-chloro-3-methoxypropane are reacted. The title compound is obtained as a slightly orange oil. Rf=0.32 (1:4 EtOAc-heptane); Rt=4.60

출처 및 근거

ORD 기록: ord-e8f831e06a64461f841a0442eed89817
출처 데이터셋: uspto-grants-2010_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07842688B2

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