참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-[2-(Trifluoromethyl)benzoyl]piperazine | HCID 16733784 | — |
| 생성물 | 1-(2-Trifluoromethylbenzoyl)piperazine hydrochloride | HCID 16733783 | 91% |
반응 단계
Ethereal HCl (30 mL) was added to piperazin-1-yl-(2-trifluoromethyl-phenyl)-methanone (5.5 g, 21.40 mmol) and the resulting mixture was stirred at 0° C. for 30 minutes. The ether was then evaporated to afford 5.7 g (91% yield) of piperazin-1-yl-(2-trifluoromethyl-phenyl)-methanone hydrochloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07842696B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_11 |
|---|
| ORD ID | ord-c33fd48809b94a23b094906311021c33 |
|---|
| 출처 메모 | uspto-grants-2010_11 |
|---|
