Triethylamine → HCID 58978005, 화합물
반응식
[CH3:1][NH:2][CH2:3][CH2:4][NH:5][C:6](=[O:15])[O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.C(N(CC)CC)C.[CH3:23][S:24](Cl)(=[O:26])=[O:25]>C(Cl)Cl>[CH3:1][N:2]([S:24]([CH3:23])(=[O:26])=[O:25])[CH2:3][CH2:4][NH:5][C:6](=[O:15])[O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1참가 물질
5
실험 절차
A solution of benzyl 2-(methylamino)ethylcarbamate (0.05 g, 0.24 mmol) in CH2Cl2 (5 mL was cooled to 6° C. and treated with triethylamine (0.1 mL, 0.72 mmol) and methanesulfonyl chloride (0.02 mL, 0.24 mmol). The reaction was warmed to room temperature and stirred overnight. The reaction was washed with 10% KHSO4, the organic layer was dried over Na2SO4, filtered and evaporated to give the product.
후처리
- washThe reaction was washed with 10% KHSO4
- dry with materialthe organic layer was dried over Na2SO4
- filtrationfiltered
- customevaporated
- customto give the product
출처 및 근거
- ORD 기록
- ord-1f44ceecbd6d49deac0bc36acf6c1302
- 출처 데이터셋
- uspto-grants-2007_10
- 특허 번호
- US07279487B2
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