Carbamic chloride, N-methyl-N-phenyl- → HCID 10150622, 화합물

HRID 1179705노트

반응식

HRID 1179705 반응식
[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([Cl:16])[C:7]=1[O:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[Cl:16][C:6]1[CH:5]=[N:4][CH:3]=[C:2]([Cl:1])[C:7]=1[O:8][C:9]1[CH:10]=[CH:11][C:12]([O:15][C:19](=[O:20])[N:18]([CH3:17])[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[CH:13][CH:14]=1

참가 물질

3

반응물 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 27265874-(3,5-Dichloro-pyridin-4-yloxy)-phenol

생성물 1

HCID 10150622HCID 10150622, 화합물

실험 절차

The title compound was prepared from 4-(3,5-dichloro-pyridine-4-yloxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was purified by preparative HPLC (41%, white crystals). HPLC-MS m/z=389.1 (M+1), Rt: 4.97 min.

후처리

  1. customThe crude product was purified by preparative HPLC (41%, white crystals)

출처 및 근거

ORD 기록
ord-40630ecaf18043a3a78e8bcb74dd70b9
출처 데이터셋
uspto-grants-2007_10
특허 번호
US07279470B2

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