Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-5-hydroxypyridine → Methyl-phenyl-carbamic Acid 6-methyl-pyridin-3-yl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-5-hydroxypyridine | HCID 14275 | — |
| 반응물 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 생성물 | Methyl-phenyl-carbamic Acid 6-methyl-pyridin-3-yl Ester | HCID 69518367 | — |
반응 단계
The title product was prepared from 3-hydroxy-6-methyl-pyridine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (79%, colourless oil). HPLC-MS: m/z=243.1 (M+1); Rt: 2.24 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07279470B2 |
| 출처 데이터셋 | uspto-grants-2007_10 |
| ORD ID | ord-6b1c434ab0af4d479c1d78728ac0c500 |
| 출처 메모 | uspto-grants-2007_10 |