Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-morpholin-4-yl-phenyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| 반응물 | 4-Morpholinophenol | HCID 80510 | — |
| 생성물 | Methyl-phenyl-carbamic Acid 4-morpholin-4-yl-phenyl Ester | HCID 10171887 | — |
반응 단계
The title product was prepared from and 4-morpholin-4-yl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was extracted with dichloromethane from citric acid (5%). The combined organic phases were evaporated and the product crystallized from ethanol (22%, crystals). HPLC-MS: m/z=313.2 (M+1); Rt: 3.75 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07279470B2 |
| 출처 데이터셋 | uspto-grants-2007_10 |
| ORD ID | ord-f6fd6e4b0ece44aca54192f6f8bc038b |
| 출처 메모 | uspto-grants-2007_10 |