Carbamic chloride, N-methyl-N-phenyl- → HCID 69519841, 화합물

반응식

[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][C:10]=1[Cl:11])[C:7](=[O:12])[N:6]([C:13]1[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=1)[C:5]2=[O:20].[CH3:21][N:22]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[C:23](Cl)=[O:24]>>[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][C:10]=1[Cl:11])[C:7](=[O:12])[N:6]([C:13]1[CH:14]=[CH:15][C:16]([O:19][C:23](=[O:24])[N:22]([CH3:21])[C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)=[CH:17][CH:18]=1)[C:5]2=[O:20]

참가 물질

반응물 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-

HCID 6915215,6-dichloro-2-(4-hydroxyphenyl)-1H-isoindole-1,3(2H)-dione

생성물 1

HCID 69519841HCID 69519841, 화합물

실험 절차

The title product was prepared from 5,6-dichloro-2-(4-hydroxy-phenyl)-isoindole-1,3-dione and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (2%,). HPLC-MS: m/z=441.1 (M+1); Rt: 5.00 min.

출처 및 근거

ORD 기록: ord-43542e135777437fbcdf6fd1d7ddffbc
출처 데이터셋: uspto-grants-2007_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07279470B2

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