참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | cis-1,2-Indandiol | HCID 20758 | — |
| 생성물 | (1R,2S)-(+)-cis-1-Amino-2-indanol | HCID 2725045 | — |
반응 단계
Cis-1,2-indandiol (1.0 g) was dissolved in acetonitrile (20 mL), cooled to -40° C., and fuming sulfuric acid (21% SO3, 0.8 mL) was added. The mixture was aged for 1 hour with gradual warming to 0° C. Water was added and the mixture heated to 80° C. for 1 hour to provide an aqueous solution of cis-1-amino-2-indanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723615 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-bb4572950e154c0d8d7ae87ec0fb230d |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
