Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Trifluoromethyl)phenylboronic acid → Methyl-phenyl-carbamic Acid 4'-trifluoromethyl-biphenyl-4-yl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Trifluoromethyl)phenylboronic acid | HCID 2734389 | — |
| 반응물 | Methyl-phenyl-carbamic Acid 4-iodo-phenyl Ester | HCID 69517304 | — |
| 생성물 | Methyl-phenyl-carbamic Acid 4'-trifluoromethyl-biphenyl-4-yl Ester | HCID 69519615 | — |
반응 단계
The title compound was prepared from methyl-phenyl-carbamic acid 4-iodo-phenyl ester and 4-trifluoromethylphenylboronic acid. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane 1:9) (42%, light brown crystals).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07279470B2 |
| 출처 데이터셋 | uspto-grants-2007_10 |
| ORD ID | ord-e3becde912d04f959c850606570f1341 |
| 출처 메모 | uspto-grants-2007_10 |