Ethyl cyclobutanecarboxylate → (1-Benzylcyclohexyl)methanol

HRID 1180746노트

반응식

HRID 1180746 반응식
[CH2:1]([C:8]1([C:14](OC)=[O:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C1(C(OCC)=O)CCC1>>[CH2:1]([C:8]1([CH2:14][OH:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 84700Ethyl cyclobutanecarboxylateHCID 15937251HCID 15937251, 화합물

생성물 1

HCID 58979707(1-Benzylcyclohexyl)methanol

실험 절차

(1-Benzylcyclohexyl)methanol was prepared as in example 5f except that methyl 1-benzylcyclohexanecarboxylate was substituted for ethyl cyclobutanecarboxylate. 1H NMR (300 MHz, DMSO-d6) δ 7.12-7.28 (m, 5H), 4.46 (t, J=5 Hz, 1H), 3.06 (d, J=5 Hz, 2H), 2.55 (s, 2H), 1.10-1.55 (m, 10H).

출처 및 근거

ORD 기록
ord-5baceb92fc7d4a028276db756296ca07
출처 데이터셋
uspto-grants-2007_10
특허 번호
US07282512B2

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