Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl 2-(3-cyanobenzylidene)-1-hydrazinecarboxylate → Tert-butyl 2-(3-cyanobenzyl)hydrazinecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl 2-(3-cyanobenzylidene)-1-hydrazinecarboxylate | HCID 69314844 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Tert-butyl 2-(3-cyanobenzyl)hydrazinecarboxylate | HCID 11831759 | 95% |
반응 단계
tert-Butyl 2-(3-cyanobenzylidene)-1-hydrazinecarboxylate (60.0 mmol) was dissolved in MeOH (250 mL) and 10% Pd/C (10 w/w %) was added. The mixture was hydrogenated for 6 h. The catalyst was filtered off and the filtrate was evaporated in vacuo to yield oily tert-butyl 2-(3-cyanobenzyl)-1-hydrazinecarboxylate which crystallized overnight.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07285547B2 |
| 출처 데이터셋 | uspto-grants-2007_10 |
| ORD ID | ord-931d97faaac748029114674e6154f725 |
| 출처 메모 | uspto-grants-2007_10 |