Potassium Carbonate → HCID 69428081, 화합물

HRID 1181773

반응식

HRID 1181773 반응식
[CH3:1][N:2]1[C:7](=[O:8])[C:6]2=[C:9]([C:23]3[CH:28]=[CH:27][N:26]=[CH:25][CH:24]=3)[N:10]([CH2:12][C:13]3[C:22]4[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=4)[CH:16]=[CH:15][CH:14]=3)[N:11]=[C:5]2[NH:4][C:3]1=[O:29].[C:30]([O:33][C:34]1[CH:39]=[CH:38][C:37]([CH2:40]Cl)=[CH:36][CH:35]=1)(=[O:32])[CH3:31].C(=O)([O-])[O-].[K+].[K+]>CN(C=O)C>[C:30]([O:33][C:34]1[CH:39]=[CH:38][C:37]([CH2:40][N:4]2[C:5]3=[N:11][N:10]([CH2:12][C:13]4[C:22]5[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=5)[CH:16]=[CH:15][CH:14]=4)[C:9]([C:23]4[CH:24]=[CH:25][N:26]=[CH:27][CH:28]=4)=[C:6]3[C:7](=[O:8])[N:2]([CH3:1])[C:3]2=[O:29])=[CH:36][CH:35]=1)(=[O:32])[CH3:31]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 1483124-(Chloromethyl)phenyl acetateHCID 1363341135-methyl-2-(1-naphthylmethyl)-3-(4-pyridinyl)-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione

생성물 1

HCID 69428081HCID 69428081, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

This compound was synthesized by the reaction of 5-methyl-2-(1-naphthylmethyl)-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione and 4-(chloromethyl)phenyl acetate using potassium carbonate as a base in DMF at 80° C.

후처리

  1. customat 80° C.

출처 및 근거

ORD 기록
ord-4900d4b6e7b74932b3efcd49b764cc43
출처 데이터셋
uspto-grants-2007_10
특허 번호
US07285558B2

연결된 노트

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