Aniline → N-phenyl-2-Dibenzofuranamine

HRID 1183195

반응식

HRID 1183195 반응식
I[C:2]1[CH:14]=[CH:13][C:5]2[O:6][C:7]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=3[C:4]=2[CH:3]=1.[NH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(OCC)(=O)C.CCCCCC>[CH:3]1[C:4]2[C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=3[O:6][C:5]=2[CH:13]=[CH:14][C:2]=1[NH:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

참가 물질

4

반응물 2

HCID 6115AnilineHCID 2233272-Iododibenzofuran

생성물 1

HCID 67204676N-phenyl-2-Dibenzofuranamine

시약·촉매·용매 1

HCID 21226206Ethyl acetate hexane용매

실험 절차

The Rf values of the object of the synthesis, 2-iododibenzofuran, and aniline were respectively 0.28, 0.59, and 0.07, which were found by silica gel thin layer chromatography (TLC) (ethyl acetate:hexane (1:10) as the developing solvent).

출처 및 근거

ORD 기록
ord-b4025fc9e8914b338ad9ffe16113d389
출처 데이터셋
uspto-grants-2014_03
특허 번호
US08664263B2

연결된 노트

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