Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenyl isocyanate → 1-Phenylaminocarbonyl-1,3-dicyclohexyl-O-(N-2-butylideneamino)-isourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenyl isocyanate | HCID 7672 | — |
| 반응물 | 1,3-Dicyclohexyl-O-(N-2-butylideneamino)-isourea | HCID 86664633 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-Phenylaminocarbonyl-1,3-dicyclohexyl-O-(N-2-butylideneamino)-isourea | HCID 86664641 | 99.9% |
반응 단계
To a solution of 1,3-dicyclohexyl-O—(N-2-butylideneamino)-isourea (Cmpd. 2) (2.93 g, 10 mmol) in dichloromethane (15 ml) is phenylisocyanate (1.19 g, 10 mmol). The mixture is stirred 1 h at room temperature and evaporated to afford 4.12 g of the title compound as a light yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08664288B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-544d12409de84665abea77945b772cb7 |
| 출처 메모 | uspto-grants-2014_03 |