Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
m-Chloroperbenzoic acid → 2-Benzenesulfinyl-6-bromo-pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 반응물 | 2-Bromo-6-phenylsulfanylpyridine | HCID 824591 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2-Benzenesulfinyl-6-bromo-pyridine | HCID 86679095 | — |
반응 단계
2-Bromo-6-phenylsulfanyl-pyridine (0.5323 g, 2 mmol) was dissolved in CH2Cl2 (20 mL) and m-chloroperbenzoic acid (0.345 g, 2 mmol) was added. The reaction was stirred at room temperature overnight then submitted to aqueous workup and purification on silica gel to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08664220B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-26914c45d55841a4a736b549738cd277 |
| 출처 메모 | uspto-grants-2014_03 |