Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylamine → H-Orn(Z)-OH
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | Fmoc-orn(Z)-OH | HCID 14999635 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | H-Orn(Z)-OH | HCID 7009570 | 199.4% |
반응 단계
The compound obtained in Example 8-5 (122.8 mg) was dissolved in DMF (2.6 ml). After the addition of diethylamine (0.26 ml), the mixture was stirred for 2 hours at room temperature. After the reaction, the solvent was removed by distillation under reduced pressure and the residue was dried under vacuum to obtain the title compound (133.5 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07098215B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-5fa1bf7313374de8b97081467abfed33 |
| 출처 메모 | uspto-grants-2006_08 |