Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,3'-(1,1,3,3-Tetramethyldisiloxane-1,3-diyl)bispropylamine → Tetramethylammonium 3-aminopropyldimethylsilanolate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,3'-(1,1,3,3-Tetramethyldisiloxane-1,3-diyl)bispropylamine | HCID 17181 | — |
| 반응물 | Tetramethylammonium Hydroxide Pentahydrate | HCID 82620 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Tetramethylammonium 3-aminopropyldimethylsilanolate | HCID 11769672 | — |
반응 단계
A 250 ml three-neck round-bottom flask equipped with a magnetic stirrer, argon inlet, and condenser with drying tube was charged with 12.4 g (0.05 mol) of 1,3-bis(3-aminopropyl)tetramethyldisiloxane, 18.1 (88.12 mmol) of tetramethylammonium hydroxide pentahydrate, and 30 ml of tetrahydrofuran. The mixture was heated under reflux in an inert gas atmosphere for 5 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08669388B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-7dc387a01e5b4d048a661473a2b2e2b4 |
| 출처 메모 | uspto-grants-2014_03 |