2-Thiophenesulfonamide → 4-Phenylbenzene-1-sulfonamide

HRID 1186654

반응식

HRID 1186654 반응식
S1C=CC=C1S([NH2:9])(=O)=O.[C:10]1([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:14][C:13]([S:16](Cl)(=[O:18])=[O:17])=[CH:12][CH:11]=1>>[C:10]1([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:14][C:13]([S:16]([NH2:9])(=[O:18])=[O:17])=[CH:12][CH:11]=1

참가 물질

3

반응물 2

HCID 728812-ThiophenesulfonamideHCID 74192(1,1'-Biphenyl)-4-sulphonyl chloride

생성물 1

HCID 50171404-Phenylbenzene-1-sulfonamide

실험 절차

5.2.3 4-biphenylsulfonamide was prepared according to the procedure for thiophene-2-sulfonamide YG1-030 except using 4-biphenylsulfonyl chloride, which afforded the title compound 642.2 mg (90.6%) as a white solid, m.p.: 223-225° C.

출처 및 근거

ORD 기록
ord-74be4dab0baf46b1b2d7ec241be8fe47
출처 데이터셋
uspto-grants-2014_03
특허 번호
US08673910B2

연결된 노트

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