Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroacetyl chloride → 6,8-Dichloro-7-ethyl-4H-benzo[1,4]oxazin-3-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroacetyl chloride | HCID 6577 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2,4-Dichloro-3-ethyl-6-aminophenol | HCID 11769652 | — |
| 생성물 | 6,8-Dichloro-7-ethyl-4H-benzo[1,4]oxazin-3-one | HCID 68912929 | 92.1% |
반응 단계
6-Amino-2,4-dichloro-3-ethylphenol (95MF2226) (0.293 g, 1.5 mmol), 2-chloroacetyl chloride (0.19 g, 1.7 mmol) and K2CO3 (0.44 g, 3.2 mmol) were mixed according to GP1 to give the title compound as a crude (95MF46) (0.34 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08680115B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-aef3c742785646b095d43abe83d69c52 |
| 출처 메모 | uspto-grants-2014_03 |