Ammonia → HCID 46932424, 화합물

HRID 1192078

반응식

HRID 1192078 반응식
[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([Cl:20])[C:7]=1[S:8][C:9]1[S:13][C:12]([C:14](O)=[O:15])=[CH:11][C:10]=1[N+:17]([O-:19])=[O:18].[NH3:21]>>[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([Cl:20])[C:7]=1[S:8][C:9]1[S:13][C:12]([C:14]([NH2:21])=[O:15])=[CH:11][C:10]=1[N+:17]([O-:19])=[O:18]

참가 물질

3

반응물 2

HCID 222AmmoniaHCID 602073175-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid

생성물 1

HCID 46932424HCID 46932424, 화합물

실험 절차

Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and ammonia (0.24 mL, 0.5 M in THF, 0.12 mmol). The title compound was obtained as a solid (4.5 mg, 12.8% yield). MS m/z: 347.80, 349.80 [M+H]+.

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-ebf4a7045c1c4370807cd7bd5beefe52
출처 데이터셋
uspto-grants-2014_03
특허 번호
US08680139B2

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