Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methoxy-N-methylbenzylamine → 5-((3,5-dichloropyridin-4-yl)thio)-N-(3-methoxybenzyl)-N-methyl-4-nitrothiophene-2-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methoxy-N-methylbenzylamine | HCID 5152225 | — |
| 반응물 | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carboxylic acid | HCID 60207317 | — |
| 생성물 | 5-((3,5-dichloropyridin-4-yl)thio)-N-(3-methoxybenzyl)-N-methyl-4-nitrothiophene-2-carboxamide | HCID 46932707 | — |
반응 단계
Prepared according to the procedure described for example 44 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (35 mg, 0.1 mmol) and 1-(3-methoxyphenyl)-N-methyl-methanamine (18.0 mg, 0.12 mmol). The title compound was obtained as a solid (18.5 mg, 38% yield). MS m/z: 484.01, 486.01 [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08680139B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-b8f352ac19194c9abe5e0baf18162e66 |
| 출처 메모 | uspto-grants-2014_03 |