Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Nitro-2-phenylethane → (E)-6-nitro-7-phenylhept-5-enal
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Nitro-2-phenylethane | HCID 80208 | — |
| 반응물 | Pentanal, 5,5-dimethoxy- | HCID 170903 | — |
| 용매 | Ethyl acetate hexane | HCID 21226206 | — |
| 생성물 | (E)-6-nitro-7-phenylhept-5-enal | HCID 58434580 | 40% |
반응 단계
Prepared according to the general procedure B from 1-(2-nitroethyl)benzene 112e (24 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (1.49 g, 40% yield) after silica gel chromatography (EtOAc/Hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08680335B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-7cf9d7b4aa8041be97c8ffed1f6d9b25 |
| 출처 메모 | uspto-grants-2014_03 |