Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pentanal, 5,5-dimethoxy- → (E)-6-nitro-7-p-tolylhept-5-enal
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pentanal, 5,5-dimethoxy- | HCID 170903 | — |
| 반응물 | 1-Methyl-4-(2-nitroethyl)benzene | HCID 11228988 | — |
| 용매 | Ethyl acetate hexane | HCID 21226206 | — |
| 생성물 | (E)-6-nitro-7-p-tolylhept-5-enal | HCID 58434561 | 35% |
반응 단계
Prepared according to the general procedure B from 1-methyl-4-(2-nitroethyl)benzene 112f (24 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (1.38 g, 35% yield) after silica gel chromatography (EtOAc/Hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08680335B2 |
| 출처 데이터셋 | uspto-grants-2014_03 |
| ORD ID | ord-2d70649003f54a99891b9c95a32471c4 |
| 출처 메모 | uspto-grants-2014_03 |