Anisole → HCID 178503584, 화합물
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[CH3:1][S:2][C:3]1[N:4]=[C:5]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=[C:6]2[N:7]=1.[C:13]1(OC)C=CC=CC=1.[F:21][C:22]([F:29])([F:28])[S:23]([O:26]C)(=[O:25])=[O:24]>C(OCC)(=O)C>[F:21][C:22]([F:29])([F:28])[S:23]([O-:26])(=[O:25])=[O:24].[CH3:13][N:7]1[C:6]2=[CH:8][CH:9]=[CH:10][CH:11]=[CH:12][C:5]2=[NH+:4][CH:3]1[S:2][CH3:1]참가 물질
5
실험 절차
First, 25 g of 2-methylthiocycloheptimidazole was added to 100 ml of anisole, and stirred under ice cooling. Then, 28 g of methyl trifluoromethanesulfonate was added dropwise and stirred under ice cooling. The mixture was further stirred at room temperature for 2 hours and 30 minutes, 200 ml of ethyl acetate was added thereto, and deposited crystals were filtered and dried.
후처리
- stirringstirred under ice cooling
- stirringThe mixture was further stirred at room temperature for 2 hours and 30 minutes
- filtrationwere filtered
- customdried
출처 및 근거
- ORD 기록
- ord-ae87d2e397e94c91a2716070b4f1ac09
- 출처 데이터셋
- uspto-grants-1989_03
- 특허 번호
- US04814265
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