Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → p-Tolylacetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Lilac acetaldehyde | HCID 61006 | — |
| 반응물 | Sodium Hypochlorite | HCID 23665760 | — |
| 생성물 | p-Tolylacetic acid | HCID 248474 | — |
반응 단계
In the like manner as Example 1, 26.4 g of p-methylphenylacetaldehyde as an aldehyde and 2.3 g of sulfuric acid were used. The oxidation was done by using 125 g of 12% aqueous solution of sodium hypochlorite at temperatures of -10° to -12° C., which was followed by the hydrogenation to obtain p-methylphenylacetic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04814494 |
| 출처 데이터셋 | uspto-grants-1989_03 |
| ORD ID | ord-a6c0e22ac83543e18b5dba56bc8d265d |
| 출처 메모 | uspto-grants-1989_03 |