1-(4-Nitrophenyl)-N-(2-phenylethyl)methanesulfonamide → 1-(4-Aminophenyl)-N-(2-phenylethyl)methanesulfonamide

HRID 1194760노트

반응식

HRID 1194760 반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][S:11]([NH:14][CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)(=[O:13])=[O:12])=[CH:6][CH:5]=1)([O-])=O>C(O)C>[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][S:11]([NH:14][CH2:15][CH2:16][C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)(=[O:13])=[O:12])=[CH:6][CH:5]=1

참가 물질

3

반응물 1

HCID 132861091-(4-Nitrophenyl)-N-(2-phenylethyl)methanesulfonamide

생성물 1

HCID 132861101-(4-Aminophenyl)-N-(2-phenylethyl)methanesulfonamide수율 94.6%

시약·촉매·용매 1

HCID 702Ethanol용매2회

실험 절차

By a procedure similar to that described in example 9(b) the product of stage (a) (7.0 g) was hydrogenated in ethanol to give the title compound as a white solid (6.0 g), m.p. 123°-125° (from ethanol).

출처 및 근거

ORD 기록
ord-4295e888bdc64f9a8e4c462d328abe1b
출처 데이터셋
uspto-grants-1989_03
특허 번호
US04816470

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