Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromocycloheptane → ethyl (2Z)-2-cycloheptyloxyimino-3-oxobutanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromocycloheptane | HCID 16992 | — |
| 반응물 | HCID 178472876 | HCID 178472876 | — |
| 생성물 | ethyl (2Z)-2-cycloheptyloxyimino-3-oxobutanoate | HCID 14864956 | 80% |
반응 단계
Ethyl (Z)-2-(hydroxyimino)-3-oxobutyrate (5.Og) was treated with cycloheptyl bromide as described in Example 13a to give the title compound as a colourless liquid (6.36 g, 80%). (Found: M+ +H, 256.1547, C13H21NO4 requires M+H 256.1550), νmax (film) 2940, 1750, 1690 cm-1 ; δH (CDCl3): 1.31 (3H, t) 1.4-2.0 (12H, m), 2.35 (3H, s) 4.32 (3H, q+m).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04816452 |
| 출처 데이터셋 | uspto-grants-1989_03 |
| ORD ID | ord-1069e163489e4cd8ae85464d03751a8d |
| 출처 메모 | uspto-grants-1989_03 |