Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodocyclooctane → ethyl (2Z)-2-cyclooctyloxyimino-3-oxobutanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodocyclooctane | HCID 13866149 | — |
| 반응물 | HCID 178472876 | HCID 178472876 | — |
| 생성물 | ethyl (2Z)-2-cyclooctyloxyimino-3-oxobutanoate | HCID 14864958 | 69% |
반응 단계
Ethyl (Z)-2-(hydroxyimino)-3-oxobutyrate (2.Og) was treated with cyclooctyl iodide as described in Example 4a, Method 1, to give the title compound as a colourless liquid (2.35 g, 69%). νmax (film) 2930, 1740, 1695 cm-1, δH (CDCl3) 1.31 (3H, t), 1.4-2.0 (14H, m), 2.38 (3H, s), 4.33 (2H, q), 4.4 (1H, m). [Mass spectrum, +ve ion, MH+ (270)].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04816452 |
| 출처 데이터셋 | uspto-grants-1989_03 |
| ORD ID | ord-126ff87843fa4fa39e94267ee1021d1d |
| 출처 메모 | uspto-grants-1989_03 |