Thionyl Chloride → HCID 54224112, 화합물

반응식

[CH2:1]([C:10]1[CH:11]=[N:12][C:13]([C:16]2[CH:24]=[CH:23][C:19]([C:20](O)=[O:21])=[CH:18][CH:17]=2)=[N:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].S(Cl)([Cl:27])=O>>[CH2:1]([C:10]1[CH:11]=[N:12][C:13]([C:16]2[CH:24]=[CH:23][C:19]([C:20]([Cl:27])=[O:21])=[CH:18][CH:17]=2)=[N:14][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 190284734-(5-Nonylpyrimidin-2-YL)benzoic acid

생성물 1

HCID 54224112HCID 54224112, 화합물

실험 절차

4-(5-n-Nonylpyrimidine-2-yl)benzoic acid (1.63 g) was heated together with excess thionyl chloride for 8 hours under reflux and thereafter, unaltered thionyl chloride was distilled off to obtain 4-(5-n-nonylpyrimidine-2-yl)benzoic acid chloride.

후처리

temperatureunder reflux
distillationunaltered thionyl chloride was distilled off

출처 및 근거

ORD 기록: ord-76d6be173910499688c3f328772855ef
출처 데이터셋: uspto-grants-1992_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05110496

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