Chlorodiphenylmethane → N-diphenylmethyl-N,N'-diethylethylenediamine

반응식

[CH2:1]([NH:3][CH2:4][CH2:5][NH:6][CH2:7][CH3:8])[CH3:2].[C:9]1([CH:15](Cl)[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[C:9]1([CH:15]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][NH:6][CH2:7][CH3:8])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

참가 물질

반응물 2

HCID 7035Chlorodiphenylmethane

HCID 67105N,N'-Diethylethylenediamine

생성물 1

HCID 13814465N-diphenylmethyl-N,N'-diethylethylenediamine수율 41.3%

실험 절차

Reaction and treatment were carried out using 21 g of N,N'-diethylethylenediamine and 7.3 g of diphenylmethyl chloride in accordance with the same procedure as in Example 3-(a), in order to obtain 4.2 g of N-diphenylmethyl-N,N'-diethylethylenediamine.

후처리

customReaction and treatment

출처 및 근거

ORD 기록: ord-29383521d2ac41c9bdf174eb4104f8dc
출처 데이터셋: uspto-grants-1992_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05112817

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