Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 1-(3,4-Dimethoxy-6-nitrobenzoyl)-4-cyclohexylcarbonyl piperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 4,5-Dimethoxy-2-nitrobenzoic acid | HCID 78690 | — |
| 반응물 | 4-Cyclohexylcarbonylpiperidine | HCID 5246602 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-(3,4-Dimethoxy-6-nitrobenzoyl)-4-cyclohexylcarbonyl piperidine | HCID 19389218 | — |
반응 단계
10.3 g of 3,4-dimethoxy-6-nitrobenzoic acid was converted to the corresponding acid chloride as described in Example 43. It was added to a solution containing 8.83 g of 4-cyclohexylcarbonylpiperidine and 4.58 g of triethylamine in 300 ml of dichloromethane. Yield 16.4 g (90%), m.p. 120°-125° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05112861 |
| 출처 데이터셋 | uspto-grants-1992_05 |
| ORD ID | ord-437dfe39a9c84fb5bfa499c0652fe18c |
| 출처 메모 | uspto-grants-1992_05 |