Methyl Acrylate → HCID 14838405, 화합물

HRID 1196004노트

반응식

HRID 1196004 반응식
[CH3:1][O:2][C:3](=[O:6])[CH:4]=[CH2:5].[NH2:7][CH2:8][CH:9]1[CH2:18][C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[O:11][CH2:10]1>CO>[CH3:1][O:2][C:3]([CH2:4][CH2:5][N:7]([CH2:5][CH2:4][C:3]([O:2][CH3:1])=[O:6])[CH2:8][CH:9]1[CH2:18][C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[O:11][CH2:10]1)=[O:6]

참가 물질

4

반응물 2

HCID 7294Methyl AcrylateHCID 4962852Chroman-3-ylmethanamine

생성물 1

HCID 14838405HCID 14838405, 화합물수율 95%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

3.03 g (35.2 mmol) of acrylic acid methyl ester are added to a solution of 2.61 g (16 mmol) of 3-aminomethylchroman in 20 ml of methanol. The reaction solution is stirred for 16 hours at 50° and, after cooling, is concentrated by evaporation in vacuo. 5.1 g (95%) of N,N-bis(2-methoxycarbonylethyl)-N-(chroman-3-ylmethyl)-amine are obtained in the form of a reddish oil.

후처리

  1. temperatureafter cooling
  2. concentrationis concentrated by evaporation in vacuo

출처 및 근거

ORD 기록
ord-f6b5bd71c31a4c1eb40ce2b89367d947
출처 데이터셋
uspto-grants-1992_05
특허 번호
US05112855

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