Acetaldehyde → HCID 14127108, 화합물

HRID 1197151노트

반응식

HRID 1197151 반응식
[S:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH:6](=O)[CH3:7].[CH:9]([C:12]1[CH:20]=[CH:19][C:15]([C:16]([NH2:18])=[O:17])=[CH:14][CH:13]=1)([CH3:11])[CH3:10]>C(O)(=O)C.S(=O)(=O)(O)O>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]([NH:18][C:16](=[O:17])[C:15]1[CH:19]=[CH:20][C:12]([CH:9]([CH3:11])[CH3:10])=[CH:13][CH:14]=1)[CH3:7]

참가 물질

5

반응물 3

HCID 177AcetaldehydeHCID 8030ThiopheneHCID 69277Benzamide, 4-(1-methylethyl)-

생성물 1

HCID 14127108HCID 14127108, 화합물수율 5%

시약·촉매·용매 1

HCID 23350293Acetic acid sulfuric acid용매

실험 절차

Thiophene (25 mmol), acetaldehyde (20 mmol) and 4-isopropylbenzamide (10 mmol) were stirred in a mixture of acetic acid/sulfuric acid (10 ml/0.2 ml) at 60° C. for one hour to obtain N-[1-(2-thienyl)ethyl]-4-isopropylbenzamide. Yield: 5%. A large part of the product was a tar-like material.

출처 및 근거

ORD 기록
ord-22e6f5daa7624279bcaab12778e7c1e6
출처 데이터셋
uspto-grants-1992_05
특허 번호
US05117000

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