Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → N'-t-butyl-N-benzoyl-N'-(2-furoyl)hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2-Furancarbonyl chloride | HCID 68242 | — |
| 반응물 | N'-tert-butylbenzohydrazide | HCID 299436 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N'-t-butyl-N-benzoyl-N'-(2-furoyl)hydrazine | HCID 15452001 | — |
반응 단계
N'-t-butyl-N-benzoylhydrazine (1 g) was dissolved in 20 ml toluene. Water (5 ml) and 50% aqueous sodium hydroxide (1.25 g) was added followed by 2-furoylchloride (0.68 g). After stirring for 7 hours at room temperature, 0.3 g 2-furoylchloride was added and the mixture stirred for a further 6 hours. The solid product, N'-t-butyl-N-benzoyl-N'-(2-furoyl)hydrazine, was removed by filtration and washed with water. m.p. 155°-175° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05117057 |
| 출처 데이터셋 | uspto-grants-1992_05 |
| ORD ID | ord-39d3585525404da5b6dc441f4856ddb6 |
| 출처 메모 | uspto-grants-1992_05 |