Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene → N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | N-(4-methoxyphenyl)-3-methyl-4-nitrobenzamide | HCID 790964 | — |
| 생성물 | N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride | HCID 13633435 | — |
반응 단계
14 g of N-(4-methoxyphenyl)-4-nitro-3-methyl benzamide in suspension in 70 ml of thionyl chloride were heated for 20 hours at reflux. The solvent was eliminated by entrainment with benzene, and after drying under reduced pressure at ambient temperature, 15 g of N-(4-methoxyphenyl)-4-nitro-3-methylbenzene carboximidoyl chloride melting towards 80° C. were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05278180 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-d6a32888520145e7b0f7ea42659d374a |
| 출처 메모 | uspto-grants-1994_01 |