Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
9-Acetylanthracene → N-octyl-beta-oxo-9-anthracenepropanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 9-Acetylanthracene | HCID 69911 | — |
| 반응물 | Octyl isocyanate | HCID 76616 | — |
| 반응물 | Lithium diisopropylamide | HCID 2724682 | — |
| 생성물 | N-octyl-beta-oxo-9-anthracenepropanamide | HCID 54127851 | — |
반응 단계
The title compound, mp 70°-72° C., was prepared from 9-acetylanthracene (5.0 g, 0.022 mol), octyl isocyanate (3.52 g, 0.022 mol), and lithium diisopropylamide (0.032 mol) using the procedure described in Example 1. Purification by flash chromatography (silica gel, 5% EtOAc/hexane) yielded 3.84 g (0.010 mol, 45.2%) of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05278326 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-8740323203a848bb8eac714a022d6c3d |
| 출처 메모 | uspto-grants-1994_01 |