Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine hydrate (1:1) → 4-Phenoxybutan-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 2-(4-Phenoxybutyl)-1H-isoindole-1,3(2H)-dione | HCID 16637597 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-Phenoxybutan-1-amine | HCID 116240 | 96.2% |
반응 단계
A mixture of N-(4-phenoxybutyl)phthalimide (7.8 g), hydrazine hydrate (7 ml) and ethanol (150 ml) was stirred for one hour under reflux. Crystalline precipitate was filtered off, then the filtrate was concentrated under reduced pressure to give 4-phenoxybutylamine (4.2 g, 95%) as an oily product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05280022 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-43de905befef4fd6a66a6a7f25f015a2 |
| 출처 메모 | uspto-grants-1994_01 |