HCID 178514060, 화합물 → 1-Aminocarbonyl-4-nitroxypiperidine

HRID 1198141노트

반응식

HRID 1198141 반응식
[NH2:1][C:2]([N:4]1[CH2:9][CH2:8][CH:7](NC([C@H]2CC[C@H](O[N+]([O-])=O)CC2)=O)[CH2:6][CH2:5]1)=[O:3].N1CCC(NC([C@H]2CC[C@H]([O:38][N+:39]([O-:41])=[O:40])CC2)=O)CC1>C(O)C>[NH2:1][C:2]([N:4]1[CH2:5][CH2:6][CH:7]([O:40][N+:39]([O-:41])=[O:38])[CH2:8][CH2:9]1)=[O:3]

참가 물질

4

반응물 2

HCID 178514060HCID 178514060, 화합물HCID 178522299HCID 178522299, 화합물

생성물 1

HCID 150688551-Aminocarbonyl-4-nitroxypiperidine수율 25%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

trans-N-(1-aminocarbonylpiperidin-4-yl)-4-nitroxycyclohexanecarboxylic acid amide from trans-4-nitroxycyclohexanecarboxylic acid piperidin-4-ylamide; yield 25% of theory; solvent: ethanol; m.p. 187°-188° C.

출처 및 근거

ORD 기록
ord-83facfb730af48f5a3af9469f3b7134f
출처 데이터셋
uspto-grants-1994_01
특허 번호
US05280031

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