Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Toluene → (4-Octyloxy-2,3-difluorophenyl)-4-propylbenzylideneamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | 4-Propylbenzaldehyde | HCID 120047 | — |
| 반응물 | 4-Octyloxy-2,3-difluoroaniline | HCID 19103699 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | (4-Octyloxy-2,3-difluorophenyl)-4-propylbenzylideneamine | HCID 53700525 | — |
반응 단계
A mixture of 0.1 mol of 4-octyloxy-2,3-difluoroaniline (prepared from the corresponding amide by a Hoffmann rearrangement), 0.1 mol of 0.1 mol of 4-propylbenzaldehyde, 0.01 mol of p-toluenesulfonic acid and 200 ml of toluene is heated at the boiling point for 2 hours using a water separator. Customary working up gives (4 -octyloxy-2,3-difluorophenyl)-4-propylbenzylideneamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05279764 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-57591a8a019f4316908f5443038ffd6d |
| 출처 메모 | uspto-grants-1994_01 |