Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propionitrile → HCID 178432489, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propionitrile | HCID 7854 | — |
| 반응물 | 1,2-Dimethylbenzimidazole | HCID 312693 | — |
| 반응물 | Disulfide, bis(2-bromoethyl) | HCID 572268 | — |
| 생성물 | HCID 178432489 | HCID 178432489 | — |
반응 단계
2.4 g of 1,2-dimethylbenzimidazole, 2.1 g of bis(2-bromoethyl) disulfide and 6 ml of propionitrile were stirred at 100 C in a sealed 20 ml reactor for 8 h. After cooling, filtration, washing with 3 times 10 ml and drying under vacuum, 2.2 g of beige solid were recovered. The analyses showed that the product was in conformity with the expected structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07727287B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-6ecb22d1266e4ad1878d98cb3b30a37b |
| 출처 메모 | uspto-grants-2010_06 |