(E)-3-(1H-Indol-7-yl)acrylonitrile → 3-(1H-Indol-7-YL)propanenitrile

HRID 1198536

반응식

HRID 1198536 반응식
[C:1](/[CH:3]=[CH:4]/[C:5]1[CH:6]=[CH:7][CH:8]=[C:9]2[C:13]=1[NH:12][CH:11]=[CH:10]2)#[N:2]>C(O)C.[Pd]>[C:1]([CH2:3][CH2:4][C:5]1[CH:6]=[CH:7][CH:8]=[C:9]2[C:13]=1[NH:12][CH:11]=[CH:10]2)#[N:2]

참가 물질

4

반응물 1

HCID 19959103(E)-3-(1H-Indol-7-yl)acrylonitrile

생성물 1

HCID 199591053-(1H-Indol-7-YL)propanenitrile

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

A solution of 7-[2-(E)-cyanoethenyl]indole (0.28 g) in ethanol (75 ml) was hydrogenated at 50 psi over 10% palladium on charcoal (0.1 g) for 4 hours. The catalyst was filtered off and the filtrate was evaporated to give the product.

후처리

  1. filtrationThe catalyst was filtered off
  2. customthe filtrate was evaporated
  3. customto give the product

출처 및 근거

ORD 기록
ord-0f8edb9087e34736b4582c2d32ffe841
출처 데이터셋
uspto-grants-1994_01
특허 번호
US05281593

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