2-(Ethylthio)ethanol → HCID 88265867, 화합물

HRID 1198643

반응식

HRID 1198643 반응식
[Na+].Cl[Au-:3](Cl)(Cl)Cl.OCCSCC.[SH:13][CH2:14][CH2:15][C:16]([NH:18][CH2:19][C:20]([OH:22])=[O:21])=[O:17]>O>[SH:13][CH2:14][CH2:15][C:16]([NH:18][CH2:19][C:20]([OH:22])=[O:21])=[O:17].[Au:3]

참가 물질

5

반응물 3

HCID 80752-(Ethylthio)ethanolHCID 27127Sodium tetrachloroaurateHCID 165505N-(1-Hydroxy-3-sulfanylpropylidene)glycine

생성물 1

HCID 88265867HCID 88265867, 화합물

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

A solution of sodium tetrachloraurate (35 g) in distilled water (200 ml) was slowly added to a solution of ethyl 2-hydroxyethyl sulphide (20.5 g) in distilled water (200 ml). Solid addition of mercaptopropionylglycine (5.21 g) followed by vigorous stirring yielded gold mercaptopropionylglycine as a white solid (yield, based on gold, 85%).

후처리

  1. customyielded

출처 및 근거

ORD 기록
ord-96d8d6cad0794406947452f09b0840cd
출처 데이터셋
uspto-grants-1994_01
특허 번호
US05281635

연결된 노트

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